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GENERAL WORKING CHARACTERISTICS
Two unusual features affect the working characteristics of niobium. First, no appreciable softening occurs below 400° C, the temperature at which niobium reacts vigorously with the atmosphere, because of its high melting pointÑapproximately 2400° C. Secondly, sheathing for protection is not practical, because the sheathing material is likely to be softer that the metal to be worked. Fortunately, niobium's cold working properties are excellent, and the metal can be easily forged, rolled, or swaged directly from the ingot at room temperature. After the cross-sectional area has been reduced by about 90 percent, annealing is necessary. Heat treatment at 1200° C for one hour causes complete recrystallization of material cold worked over 50 percent. The annealing process must be performed in an inert gas or in a high vacuum at pressures below 1 x 10 -4 Torr. The use of a vacuum is preferred, because it is difficult to ensure the purity of inert gas. It is also less expensive to use vacuum furnaces for these operations. Niobium is well suited to deep drawing, and the metal may be cupped and drawn to tube, although special care must be taken with lubrication. The sheet metal can be formed easily by general sheet metal working techniques. The low rate of work hardening facilitates these operations by reducing springback.
MACHINING

Niobium may be machined by the usual techniques although, due to the tendency of the material to gall, special attention should be paid to tool angles and lubrication.

TURNING
Lathe turning is best carried out with High Speed Steel tools, using air, soluble oil, Rapid-Tap, or other suitable products for cooling and lubricating. This material turns very much like lead or soft copper. It must be sheared and the chip allowed to slide off the tool surface. If any buildup of the material is allowed, the pressure will break the cutting edge and ruin the tool. Carbide tooling should be used only for fast, light cuts, with a depth of .010 to .015 inches, to work efficiently. Tooling recommendations are given in Table 3, which contains data applying to High Speed Steel and Carbide tools. Contact Wah Chang for special tooling information and technical assistance.

TABLE 3 - TOOLING RECOMMENDATIONS for MACHINING Nb

Approach AngIe 15° to 20°
Side Rake 30° to 35°
Side and End Clearance
Plan Relief AngIe 15° to 20°
Nose Radius 0.020" to 0.030"
Cutting Speed 60 to 80 feet/minute with HSS
  250 to 300 feet/minute with carbide
Feed, Roughing 0.008" to 0.01 2"/revolution
Feed, Finishing 0.005" maximum/revolution
Depth of Cut 0.030" to 0.125"

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INDEX  •  CORROSION RESISTANCE PROPERTIES  •  FABRICATION   
NIOBIUM PRODUCTS     SPECIFICATIONS of NIOBIUM   
NIOBIUM ELECTRONICS APPLICATIONS