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NIOBIUM-TITANIUM ALLOY, CONT., P. 3

6. Internal Structure

6.1 Inclusions.The finished product of a size of 5/8" diameter or less shall be free of inclusions in excess of 0.013 inch (equivalent diameter) as determined by ultrasonic inspection between 1/2Ó and 5/8" diameter. Finished product of a size greater than 5/8" and less than 2" diameter shall be free of inclusions in excess of 3% of the product diameter or 0.032 inch, whichever is smaller. At manufacturer's discretion ultrasonic inspection may be performed at the finished size.

6.2 Defects. Defects such as cracks, laminations, and other ruptures shall be determined by ultrasonic examination per 6.1.

6.3 Grain Size. The grain size of each lot of finished product of 5/8" inch diameter or less shall be ASTM No. 6 or finer. The grain size shall be determined using the applicable provisions of ASTM E 112. Grain size of larger diameter product (greater than 1/2 inch) shall be specified in the purchase order.

7. Manufacture

7.1 Melting. The melting process shall be a process that has been established by the Supplier for melting niobium alloy containing 45/48 wt. % titanium for use in manufacturing wire for superconducting applications.

7.2 Working. Each ingot shall be reduced during manufacturing by a process that has been established by the Supplier for working niobium alloy containing 45/48 wt. % titanium for use in manufacturing wire for superconducting applications.

7.3 Heat Treatment. Heat treatment shall be accomplished in a manner which will preclude contamination that might cause a violation of the chemistry requirements and will ensure that each item in the lot being heat treated has essentially the same heat treated properties.

7.4 Fabrication A. Manufacturing, dependent on ingot size, shall be in accordance with processes established and shall have a minimum of 75% reduction from ingot to billet. Material shall then be cold reduced by further work, a minimum of 50%.

8. Analytical Chemistry Procedures

The procedures for analyzing to the chemistry requirements of this specification shall be in accordance with standards considered industrially acceptable for the specified alloys.

9. Nondestructive Testing Requirements

All products shall be examined nondestructively in accordance with the following requirements and shall comply with the specified acceptance criteria.

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